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Synthesis of isoindolinone phosphonates and their related derivatives by multicomponent reaction

Rávai, Bettina ; Popovics-Tóth, Nóra ; Tajti, Ádám ; Bálint, Erika

Phosphorus, Sulfur, and Silicon and the Related Elements: ICPC-23: 23rd International Conference on Phosphorus Chemistry; Guest Editors:Professor Jozef Drabowicz; Professor Piotr Kiełbasiński and Professor Tomasz Cierpiał, 2022, Vol.197 (5-6), p.599-600

Taylor & Francis

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  • Título:
    Synthesis of isoindolinone phosphonates and their related derivatives by multicomponent reaction
  • Autor: Rávai, Bettina ; Popovics-Tóth, Nóra ; Tajti, Ádám ; Bálint, Erika
  • Assuntos: continuous flow reactor ; in situ FT-IR spectroscopy ; isoindolinone phosphine oxides ; isoindolinone phosphonates ; Kabachnik-Fields reaction ; N-heterocycles
  • É parte de: Phosphorus, Sulfur, and Silicon and the Related Elements: ICPC-23: 23rd International Conference on Phosphorus Chemistry; Guest Editors:Professor Jozef Drabowicz; Professor Piotr Kiełbasiński and Professor Tomasz Cierpiał, 2022, Vol.197 (5-6), p.599-600
  • Descrição: An efficient catalyst-free microwave (MW)-assisted method was elaborated for the batch and continuous flow synthesis of N-alkyl-isoindolinone phosphonates by the three-component reaction of 2-formylbenzoic acid, primary amines and various dialkyl phosphites. The reaction was also extended to various secondary phosphine oxides and primary amines, as well. In order to obtain more information about the condensation, the reaction mechanism was also studied by in situ FT-IR spectroscopy.
  • Editor: Taylor & Francis
  • Idioma: Inglês
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  • Realização: ABCD-USP USP   Logos de Redes Sociais: Freepik

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